Synthesis of Sodium Ethoxide A solution of sodium ethoxide was prepared by adding freshly cut sodium (2.72 g, 118 mmoles)…
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Preparation of benzyl bromide Benzyl bromide, as in case with benzyl chloride, is prepared by action of bromine on toluene.…
Preparation of phenylmagnesium bromide Phenylmagnesium Bromide: The formation of the Grignard reagent from bromobenzene and magnesium in ether, is difficult from…
Synthesis of Acetylferrocene Acetylferrocene: A mixture of 93.0 g (0.5 mol) of ferrocene, 250 ml of acetic anhydride and 20…
Preparation of Benzonitrile Benzonitrile: A solution of benzenediazonium chloride is prepared by dissolving 20 ml (or 20.5 g) aniline in…
Synthesis of Sorbitan Oleate To 1000 ml of a phosphate buffer having a pH of 7.3 were added 4.93 g…
Preparation of Aluminium Iodide Aluminium Iodide: Eighteen grams of iodine, heated to about 180°C are sublimed over 60 g of aluminum…
Preparation of Cyclopentanol / cyclopentanone Cyclopentanol: 88.5 ml (or 84.1 g) of Cyclopentanol / cyclopentanone are dissolved in the mixture of…
Synthesis of Sodium Ethoxide Sodium Ethoxide: A solution of sodium ethoxide was prepared by adding freshly cut sodium (2.72 g,…
Preparation of p-benzoquinone (benzoquinone; quinone) Benzoquinone: Quinone usually is prepared by the oxidation of aniline in acid solution with sodium dichromate.…